Acta Chimica 21. (1959)

1. szám - PHYSIKALISCHE CHEMIE - T. Lengyel: Energy Dependence of the Back-scattering Factor of Absolute Beta Counting

52 LENGYEL: ENERGY DEPENDENCE In the case of measurements carried out with the GM tube, the three factors fw> fti and/s among the data of equation (1) may be considered as energy-depending beside the back-scattering factor. A definition for the back-scattering factor is given by the quotient (2) where I' is the observed activity by applying a back-scattering medium and II" the observed activity without applying a back-scattering medium. From relation (2) it is seen that in the case of each isotope a possibility is given to determine fB by the quotient of the results of two measurements. Since all the conditions of the measurements are identical, except for the back­­scattering and isotopes serving as radiation sources, any factor which does not depend on energy will be eliminated at evaluation in consequence of the division ; fw, one of the energy depending factors can be computed with the knowledge of the radiation energy and experimental conditions, fs and fH, however, are practically regarded as being equal to 1 [1, 5, 10] by choosing convenient experimental conditions, of which mention will be made later. Measuring device Data obtained with the Geiger—Müller tube with a mica end-window, which was used in the experiments, are given in Table I. Table I Technical data of the GM tube applied To the other accessories necessary for measurements, the GM tube was connected with threaded fitting parts made of plexi-glass. In each case the radiation source was applied to a 0,11 mg cm-2 thick film made of Zapon lacquer. The small nominal atomic number of the lacquer and its thinness rendered it possible to disregard practically any back-scattering, when this “infinitely thin” carrier layer was applied. To reduce the value of factor/н to 1 and to improve the geometrical condi­tions of measurements, the distance between the radiation source and GM tube had to be little — merely 8 mm. With absorption measurements of absorbent sheets were directly fitted to the end-window, so as to avoid secondary scattering. Also the back-scattering medium was directly fitted to the lower side of the film holding the radiation source. The back-scattering medium was made of foils with a smooth surface.* Working voltage ....................... Length of plateau...................... Slope of plateau per 100 У Thickness of end-window Dimension of the end-window Dead-time .................................. 1450 Y 300 У (1350—1650) 3% 1,9 mg cm-2 3,14 cm2 (0 = 20 mm) 130 jiisec •The applied isotopes were imported from the Soviet Union by the Atomic Energy Commission of Hungary. Acta Chim. Hung. Tomus 21. 1959

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